Advanced TEM and SEM methods applied to 3D Nano- and microstructural investigations of Ni4Ti3 precipitates in Ni-Ti (SMA)

Dominique Schryvers, Wim Tirry, Shanshan Cao

Onderzoeksoutput: Hoofdstuk in Boek/Rapport/CongresprocedureConferentiebijdragepeer review

Samenvatting

Two different kinds of experimental approaches yielding three-dimensional structural information on metastable semi-coherent precipitates are demonstrated. By combining high-resolution images from two independent viewing directions a full description of the strain field surrounding a nano-sized Ni4Ti3 precipitate in Ni-Ti can be obtained. The principal axes and strains correlate well with the transformation strain of the observed R-phase transformation close to the precipitate. Using a slice-and-view procedure in a FIB/SEM dual-beam instrument, a three-dimensional voxel dataset is produced from which morphological and distributional information on the same precipitates can be obtained yielding new insight into the particular transformation paths of these alloys, relevant for their functional behaviour.

Originele taal-2Engels
TitelSolid-Solid Phase Transformations in Inorganic Materials
UitgeverijTrans Tech Publications Ltd
Pagina's229-235
Aantal pagina's7
ISBN van geprinte versie9783037851432
DOI's
StatusGepubliceerd - 2011

Publicatie series

NaamSolid State Phenomena
Volume172-174
ISSN van geprinte versie1012-0394

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